SOLID-LIQUID EXTRACTION (PACKED BED TYPE) MAKE : CREATIVE LAB MODEL NO: CLMT-05, SOLID-LIQUID EXTRACTION BONOTTO TYPE MAKE MODEL:CLMT-04, SPRAY TOWER MAKE :CREATIVE LAB MODEL NO: CLMT-03, LIQUID-LIQUID EXTRACTION IN A PACKED TOWER, DOUBLE EFFECT EVAPORATOR MAKE : CREATIVE LAB MODEL NO:CLHT-30, manufacturers suppliers in India

DOUBLE EFFECT EVAPORATOR MAKE : CREATIVE LAB MODEL NO:CLHT-30

DESCRIPTION:

Evaporation deals with the concentration of a non-volatile solute from a solution by the removal of required amount of volatile solvent. Usually the solvent is water. By vaporizing a part of the solvent, useful product i.e. the concentrated solution or thick liquor is produced and the vapour is discarded. Long tube evaporators are usually used for the concentration of foamy liquids. The set-up consists of stainless steel tubes surrounded by a stainless steel jacket and fitted with accumulator. Dilute solution is feed to tubes. Steam from a steam generator is supplied to shell to concentrate the dilute feed solution to a desired level. The jacket is fitted with a steam trap and the condensate is collected at the end of trap. The vapours of volatile solvent are condensed in a shell & tube type condenser and the balance non-volatile solute collected in the accumulator is recycled through the evaporator.

EXPERIMENTATION:

To concentrate a solution and to evaluate the following at steady state:

Material and Heat Balance.

Economy and the capacity of the evaporator.

Overall heat transfer co-efficient.

UTILITIES REQUIRED:

Water supply 5 lit/min (approx.) and Drain.

Electricity Supply : 1 Phase, 220 V AC, 4 kW.

Required Chemicals.

TECHNICAL DETAILS

Evaporator Material stainless steel

Shell Dia - 75mm, Length - 750mm,

Tubes Dia - 12mm, Length - 750mm

Feed Circulation By Gravity feed

Feed Tank Material stainless steel, Capacity 25 Ltrs.

Flow Measurement Rotameters (One each for feed & cold water).

Steam Generator Made of stainless steel provided with Pressure Gauge & Level Indicator, Safety valve and drain etc. & insulated with ceramic wool and cladding with Aluminium foil.

Piping Stainless Steel and PVC, size ¼”.

Condenser Shell & Tube type made of Stainless Steel.

Bottom Product Tank Made of Stainless Steel, capacity 10 Ltrs.

Water Supply Tank Made of Stainless Steel, capacity 50 Ltrs.

For Condenser

Pump FHP capacity

Heaters Nichrome wire heater.

Control panel comprises of

Digital Temp. Controller 0-199.90C, (For Steam Generator)

Digital Temp. Indicator 0-199.90C, with multi-channel switch.

Temp. Sensors RTD PT-100, Standard make On/Off switch, Mains Indicator etc.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole set-up is well designed and arranged on a good quality painted structure.

LIQUID-LIQUID EXTRACTION IN A PACKED TOWER

DESCRIPTION:

The set-up consists of a glass column packed with Rasching rings. Continuous counter current contacts between the solvent and solute phases is made, which results into extract and raffinate streams. Flow meters (Rotameters) are used to note the flow of solvent & solute respectively. The continuous and dispersed phase streams are metered and derived from separate containers. The total set-up is housed in a well-designed rigid structure. The structure also supports tanks, piping, Rotameters, panel and other units.

EXPERIMENTATION:

To determine overall mass transfer co-efficient based on continuous & dispersed phase.

To determine individual “Height of Transfer Unit” based on continuous & dispersed phase.

UTILITIES REQUIRED:

Water Supply

Compressed Air Supply at 2 bar, 4 CFM.

Drain.

Required Chemicals & Laboratory Glassware.

TECHNICAL DETAILS:

Extraction Column Material Borosilicate Glass,

Dia 55 mm, Height 750 mm (approx).

Packing Rasching Rings, Material Borosilicate Glass,

Feed Tanks Material Stainless Steel, Cap. 20 Ltrs. (2 Nos.)

Extract & Raffinate Tanks Material Stainless Steel, Cap 10 Ltrs.

Feed Circulation By Compressed Air.

Pressure Regulator 0-2 kg/cm2.

Pressure Gauge Bourdon type, 0-2 kg/cm2.

Flow Measurement Rotameters (One each for solvent & solute)

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

Special arrangement for changing height of interface zone is done.

SPRAY TOWER MAKE :CREATIVE LAB MODEL NO: CLMT-03

DESCRIPTION

The experimental set-up of Spray Tower consists of a glass column provided with necessary accessories. It operates on a semi-batch mode. Fine spray nozzle is fitted at the top. Feeds are metered by Rotameters and derived from separate feed tanks. The liquid-liquid interface can be maintained by controlling the flow rate of extract with the help of needle valve provided on Rotameter. Total set-up is housed in a rigid structure. The structure also supports tanks, piping, Rotameters and other unit.

EXPERIMENTATION:

To study the effect of the dispersed phase flow rate on overall volumetric mass transfer coefficient.

Dispersed phase hold-up study.

UTILITIES REQUIRED:

Compressed Air Supply at 2 Bar, 0.5 CFM.

Water Supply

Drain.

Required Chemicals & Laboratory Glassware.

TECHNICAL DETAILS:

Extraction Column

Material Borosilicate Glass

Diameter 45 mm (approx).

Height 750 mm (approx).

Feed Tank

Material Stainless Steel

Capacity 20 Ltrs.

Quantity 2 Nos.

Extract & Raffinate Tanks

Material Stainless Steel

Capacity 10 Ltrs.

Quantity 2 Nos.

Feed Circulation By Compressed Air

Pressure Regulator 0-2 kg/cm².

Pressure Gauge Bourdon type, 0-2 kg/cm2.

Flow Measurement Rotameters (One each for Solvent & Solute)

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

Special arrangement for changing height of interface zone is done.

The whole set-up is well designed and arranged in a good quality painted structure.

SOLID-LIQUID EXTRACTION BONOTTO TYPE MAKE MODEL:CLMT-04

DESCRIPTION:-

The setup consists of Bonnotto type extractor of slotted circular plates arranged one above the other in opposite radial opening. The solids are introduced at the top through a hopper spread over the top plate by a rack and pushed to slot to fall to the next plate below and so on to the bottom of the column. The solvent is introduced near the bottom of the column and it flow upward counter-currently to the solids. A pump supplies the solvent and flow rate is monitored by means of a Rotameter. At the bottom of column a screw conveyor arrangement is done to remove the extracted solids driven by means of an electric motor. Solvent feed tank is kept in a bath fitted with heater and digital temperature controller is used to maintain the constant temperature.

EXPERIMENTATION:

To determine the efficiency of a continuous counter-current Solid-Liquid Extraction system.

UTILITIES REQUIRED:

Electricity Supply : 1 Phase, 220 V AC, 3 kW.

Solvent: 50 ltrs.

Solid: 30 kg.

TECHNICAL DETAILS:

Extraction Column Material Stainless Steel Dia 150 mm, Height 750 mm (approx)

Plates Material Stainless Steel, with Radial opening.

Mixer Stainless Steel Impellers fitted on Stainless Steel Shaft coupled to a motor & reduction gear box.

Screw Conveyor Material Stainless Steel, Compatible capacity, housed in GI Pipe and driven by a motor & reduction gear box.

Solvent Flow Measurement Rotameter.

Solvent Tank Made of Stainless Steel, Capacity 30 Ltrs. Double wall.

Feed circulation Magnetic Pump made of Polypropylene to Circulate solvent. Maximum working temperature is 60°C.

Heater Nichrome wire heater.

Feed Hopper Suitable capacity.

Filtration Sieve Material Stainless Steel.

Receiving Tank for Material Stainless Steel.

Extracted solid waste Compatible capacity.

Temperature Sensor RTD PT-100 type.

Control panel comprising of

Digital Temp. Controller 0-200°C, For Feed Tank

Standard make on/off switch, Mains Indicator etc.

SOLID-LIQUID EXTRACTION (PACKED BED TYPE) MAKE : CREATIVE LAB MODEL NO: CLMT-05

DESCRIPTION:-

This setup is designed to study the performance characteristics of Solvent extraction of a particular component from a packed bed of solid material. The apparatus allows study of such systems aswater/inorganic salts, water/sugar bed, methylene chloride/vegetable oil etc. The glass column is fitted with SS mesh to support the solid material. The solvent is introduced near the bottom of the column and it flows upward counter-currently to the solids. A pump supplies the solvent and flow rate is monitored by means of a Rotameter. Solvent feed tank is kept in a bath fitted with heater and digital temperature controller is used tomaintain the constant temperature.

EXPERIMENTATION:

To study the effect of various system parameters like, solvent temperature, solvent rate and particle size on the %age recovery of oil from solid.

UTILITIES REQUIRED:

Electricity Supply : 1 Phase, 220 V AC, 1.5 kW.

Solvent: 30 ltrs.

Solid : 10 kg. Table for setup support

TECHNICAL DETAILS:

Extraction Column Material Borosilicate Glass.

Dia 80 mm, Height 500 mm (approx.)

Solvent Flow Measurement Rotameter.

Solvent Tank Made of Stainless Steel, Capacity 30 Ltrs.

Double wall.

Solvent circulation Magnetic Pump made of Polypropylene to

Circulate solvent.

Maximum working temperature is 60°C.

Heater Nichrome wire heater.

Receiving Tank Material Stainless Steel, Compatible capacity.

Temperature Sensor RTD PT-100 Type.

Control panel comprising of

Digital Temp. Controller 0-199.9°C (For Feed Tank)

Standard make on/off switch, Mains Indicator etc

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SOLID-LIQUID EXTRACTION (PACKED BED TYPE) MAKE : CREATIVE LAB MODEL NO: CLMT-05 SOLID-LIQUID EXTRACTION BONOTTO TYPE MAKE MODEL:CLMT-04 SPRAY TOWER MAKE :CREATIVE LAB MODEL NO: CLMT-03 LIQUID-LIQUID EXTRACTION IN A PACKED TOWER DOUBLE EFFECT EVAPORATOR MAKE : CREATIVE LAB MODEL NO:CLHT-30