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BUBBLE CAP DISTILLATION COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-06
DESCRIPTION:                                                                                                                       
The column is made of Stainless Steel with seven plates for mounting the bubble caps. Each plate is provided with one bubble cap. An electrically heated reboiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by cooling water supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation provided for pressure & temp. measurement wherever necessary.
EXPERIMENTATION:
To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known number of theoretical plates.
To operate the column under total reflux condition and estimate the minimum number of theoretical plates required.
UTILITIES REQUIRED:
Water Supply 2 LPM at 5 m head.
Drain.
Electricity Supply: 1 Phase, 220 V AC, 6 kW.
Required Chemicals.
Refractometer for analysis.
TECHNICAL DETAILS:
Distillation Column Material Stainless Steel, Dia 110mm, seven plates.
Pressure Gauge Bourdon type
Rotameter For cooling water flow rate measurement.
Steam Generator   Made of Stainless Steel, provided with Pressure Gauge & Level Indicator, Safety valve & insulated with ceramic wool and cladding with Aluminium       foil.
Reflux Divider Special arrangement to change R/D ratio automatically.
Condenser Shell & Tube type made of Stainless Steel.
Bottom product tank capacity 5 Ltrs.
Distillate tank capacity 5 Ltrs.
Heater Nichrome wire heater.
Temp. Sensors RTD PT-100 type (12 Nos)
Control panel comprises of           :
Digital Temp. Controller  0-199.9°C, For Reboiler. (Nutronics Make)
Digital Temp. Indicator 0-199.9oC, with multi-channel switch (Nutronics Make)
With Standard make on/off switch(L & T makes), Mains Indicator etc.
 
 

PACKED BED DISTILLATION COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-08

DESCRIPTION:
The column is made of Stainless Steel material packed with Borosilicate Glass rasching rings. An electrically heated reboiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by circulating cooling water, supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temp. measurement wherever necessary.
EXPERIMENTATION:
To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known packed height.
To operate the column under total reflux condition and estimate the HETP for the packing.
UTILITIES REQUIRED:
Water Supply 2 LPM at 5 m head.
Drain.
Electricity Supply: 1 Phase, 220 V AC, 6 kW.
Required Chemicals.
Refractometer for analysis.
TECHNICAL DETAILS:
Distillation Column  Material Stainless Steel , Dia 80mm, Length 900mm (approx).
Packing Material Borosilicate Glass Rasching Rings.
Pressure Gauge      Bourdon type
Rotameter For cooling water flow rate measurement.
Steam Generator Made of Stainless Steel, provided with Pressure Gauge & Level Indicator, Safety valve & insulated with ceramic wool and cladding with         Aluminium foil.
Reflux Divider       Special arrangement to change R/D ratio automatically.
Condenser Shell & Tube type made of Stainless Steel.
Bottom Product Tank Made of Stainless Steel, capacity 5 Ltrs.
Distillate tank Made of Stainless Steel, capacity 5 Ltrs.
Heaters Nichrome wire heater.
Temp. Sensors RTD PT-100 type (7 Nos)
Control panel comprises of  
Digital Temp. Controller 0-199.9°C, (For Re-boiler) (Nutronics Make)
Digital Temp. Indicator      0-199.90C, with multi-channel switch (Nutronics Make)
With Standard make on/off switch, Mains Indicator etc.

 

SIMPLE BATCH DISTILLATION MAKE : CREATIVE LAB MODEL NO: CLMT-10
DESCRIPTION:                                                                                               
The equipment consists of a distillation still made of stainless steel. the feed in the still is heated externally by heater. The vapours form the top of the vessel are condensed in the type condenser by circulating cooling water. Temperature of the feed mixture is controlled by means of a digital temp. controller. The condensate is collected in a receiver made of stainless steel.
EXPERIMENTATION:
To study the characteristics of Simple Distillation.
To verify of Reyleigh’s Equation
UTILITY REQUIRED:
Water Supply 2 LPM at 5m head.
Drain.
Electricity Supply: 1 Phase, 220 V AC, 3 kW.
Required Chemicals.
TECHNICAL DETAIL:
Flow measurement Rotameter for cold water for condenser
Distillation still Made of Stainless Steel, capacity 5 ltrs. Insulated with  ceramic wool and cladding with Aluminum foil.
Condenser Concentric Tube type made of Stainless Steel
Distillate tank Made of Stainless Steel, capacity 2 Ltrs.
Heater Nichrome wire heater.
Control panel comprises of  
Digital Temp. Controller 0-199.9°C, RTD PT-100 type (For Steam Generator)
Digital Temp. Indicator 0-199.90C with multi-channel switch.
Temp. Sensors   RTD PT-100 type With Standard make on/off switch, Mains Indicator
Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus
The whole set-up is well designed and arranged in a good quality painted structure..
 
 
 

ABSORPTION IN SIEVE PLATE COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-11
DESCRIPTION:
The set up consists of a column fitted with perforated plates. Liquid is fed at the top of the column through distributor. The solute gas and air are measured separately, mixed in a mixing chamber and then passed through the perforated plates vertically upward and absorbed in liquid. All the flow rates can be independently varied to simulate different conditions. Liquid Sample can be taken out from the bottom of the column for analysis.
EXPERIMENTATION:
To study absorption of CO2 in aqueous NaOH solution in a sieve plate column.
To determine the gas phase mass transfer co-efficient, KG a
UTILITIES REQUIRED:
Water Supply
Floor Drain.
Required Chemicals & Laboratory Glassware.
Compressed air supply at 2 bar, 4 CFM.
CO2 cylinder with control valve, pressure regulator and Pressure gauges
TECHNICAL DETAILS:
Column Material Stainless Steel. Dia 80mm, Length 1000mm (approx.) One section of column is provided of Borosilicate glass to visualize the rocess
Plates Perforated Plates made of Stainless Steel (7 Nos.)
Feed Circulation By compressed air.
Pressure Regulator  0-2 kg/cm².
Pressure Gauge  Bourdon type
Feed Tank Material Stainless Steel, Capacity 20 Ltrs.
Flow Measurement Rotameters (One each for feed, air & CO2).
Collecting Tank Material Stainless Steel, Capacity 10 Ltrs.
Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus 
The whole set-up is well designed and arranged in a good quality painted structure.
 
 
 

ABSORPTION IN PACKED BED MAKE : CREATIVE LAB MODEL NO:CLMT-12
DESCRIPTION:
The set up consists of a glass column packed with Rasching rings. Liquid is fed at the top of the column through distributor. The solute gas and air are measured separately, mixed in a mixing chamber and then passed through the packed column vertically upward and absorbed in liquid. All the flow rates can be independently varied to simulate different conditions. Liquid sample can be taken out from the sampling point at the bottom of the column for analysis.
EXPERIMENTATION:
To determine the number of transfer units, Height of transfer unit and overall mass transfer co-efficient for the given system.
UTILITIES REQUIRED:
Water Supply
Floor Drain.
Required Chemicals & Laboratory Glassware.
Compressed air supply at 2 bar, 4 CFM.
CO2 cylinder with control valve, pressure regulator and Pressure gauges
TECHNICAL DETAILS:
Column Borosilicate Glass Dia 55 mm, Length 750 mm (approx.)
Packing Borosilicate Glass Rasching Ring
Feed Circulation By compressed air.
Pressure Regulator 0-2 kg/cm².
Pressure Gauge Bourdon type
Feed Tank Material Stainless Steel, Capacity 20 Ltrs.
Flow measurement Rotameters (One each for feed, air & CO2).
Collecting Tank Material Stainless Steel, Capacity 10 Ltrs.
Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus
The whole set-up is well designed and arranged in a good quality painted structure.
 
 

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ABSORPTION IN PACKED BED MAKE : CREATIVE LAB MODEL NO:CLMT-12    ABSORPTION IN SIEVE PLATE COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-11    SIMPLE BATCH DISTILLATION MAKE : CREATIVE LAB MODEL NO: CLMT-10    PACKED BED DISTILLATION COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-08    BUBBLE CAP DISTILLATION COLUMN MAKE : CREATIVE LAB MODEL NO:CLMT-06    
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